THE MILLIMETER AND SUBMILLIMETER WAVE SPECTRA OF PROTONATED AND DEUTERATED NITROUS OXIDE

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1987

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Ohio State University

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A magnetically confined glow discharge has been used to produce protonated and deuterated nitrous oxide in a mixture of $N_{2}O, H_{2}/O_{2}$ and Ar. A total number of 63 rotational lines for $HON^{+}_{2}$ and 89 for $DO N^{+}_{2}$ characterized respectively by $5 \leq J \leq 18, K_{a} \leq 4$ and $0 \leq J \leq 27, K_{a} \leq 7$ have been observed in the 130 - 405 GHz frequency range. These lines belong to a-type $r_{p}$ - branches and to b-type $r_{R} \_ ^{q}_{R} -$ and $r_{p}$ - branches. From the analysis of these two types of spectrum, accurate molecular parameters have been derived which are in good agreement with recent IR experiments on $HON^{+}_{2}$ (1). The values obtained for the A rotational constant: $\begin{array}{lll}A_{o} = 625957.716 (52) MHz for HON^{+}_{2}\\ \quad \qquad and A_{o} = 349107.385 (14) MHz for DON^{+}_{2}\end{array}$ confirm the recent results of ab initio calculations leading to the conclusion that the preferred site of protonation is at the oxygen atom.

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(1) T. Amano, Chem. Phys. Lett., 127, 101 (1986).
Author Institution: Laboratoire de Spectroscopie Hertzienne associ\'e au CNRS, Universit\'e de Lille I; Laboratoire de Spectroscopie Hertzienne associ\'e au CNRS, Herzberg Institute of Astrophysics

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