OBSERVATION OF THE CH STRETCH BAND OF $CH^{-}_{3}$

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1997

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Ohio State University

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{Ab initio} calculation predict that protonated methane, $CH^{+}_{5}$, has three low energy structures that are practically equal in energy and that barriers separating their 120 equivalent minima are $low^{m}$. Thus $CH^{+}_{5}$ provides a new prototype of spectroscopic specimen in which the five equivalent protons are attached to the central carbon $atom^{n}$. We have observed, using our difference frequency spectrometer and the velocity modulation technique, a weak but rich spectrum of a carbocation containing one carbon. We believe they are transitions of $CH^{+}_{5}$ due to the formally forbidden CH stretch band based on their plasma chemical behavior and agreement with the conclusion of predissociation spectroscopy of $CH^{+o}_{7}$. A preliminary observational result will be reported.

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$^{m}$P. R. Schreiner, S.-J. Kim, H. F. Schaefer III, and P. von Ragu\'e Schieyer, {J. Chem. Phys}. 99, 3716 (1993) $^{n}$P.R. Bunker. {J. Mol. Spectrosc}. \textbf{176}, 297 (1996) $^{o}$D.W. Boo and Y. T. Lee, {Chem. Phys. Lett}. \textbf{211}, 358 (1993)
Author Institution: Department of Chemistry, The University of Chicago

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