PHOTOCHEMISTRY OF MONOCHLORO COMPLEX OF COPPER (II) IN SOLUTION BY MEANS OF TRANSIENT ABSORPTION TIME-RESOLVED ULTRAFAST SPECTROSCOPY

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2010

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Ohio State University

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Abstract

The photodissociation mechanism of copper (II) chloro complexes in methanol is studied by means of ultrafast broadband time-resolved deep-UV/UV/vis spectroscopy using $[Cu^{II}(MeOH)_5 Cl]^+$ as a model molecule. Upon 255 nm excitation, the majority of $[Cu^{II}(MeOH)_{5}Cl]^{+}$ dissociate to form chlorine atoms $Cl^{.}$ and penthacoordinate copper(I) solvated complexes $[Cu^{I}(MeOH)_{5}]^{+}$, which is followed by recombination back to the parent molecules. A three body-disscoation in which the nascent $[Cu^{I}(MeOH)_{5}]^{+}$ fragment undergoes a methanol-ligand loss is observed to be of minor importance. The solvent influence on the photoreaction will be discussed.

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Author Institution: Bowling Green University, Department of Chemistry and Center for Photochemical Sciences, Bowling Green, Ohio 43403

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