INDUCED INFRARED ABSORPTION OF $H_{2}$ IN SOLID $C_{60}$

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2002

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Ohio State University

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We use infrared spectroscopy to observe the quantum dynamics of molecular hydrogen trapped within the interstitial sites of the $C_{60}$ lattice. These spectra form the first observation of infrared activity induced by the $C_{60}$ intermolecular potential. They also reveal the first evidence for distinct side-bands (at +/- $127 cm^{-1}$) associated with the translational motion of the trapped species. On exposure of $C_{60}$ to high pressure $H_{2}$ the induced modes grow in intensity over the course of a few hours as the $H_{2}$ slowly diffuses into the octahedral interstitial sites. Despite the fact that the fundamental $H_{2}$ vibrational mode occurs highly red-shifted ($54 cm^{-1}$) relative to the gas phase the location of the rotatioanal side-bands indicates almost complete rotational freedom of the trapped $H_{2}$. Most surprisingly the spectra contain weak central zero-phonon modes which should not be activated by a potential with true octahedral symmetry. These zero-phonon modes show a sudden decrease in intensity on cooling through the $C_{60}$ orientational phase transition at 260 K. We speculate that this may be the result of freezing out of a quasi fluid like surface layer within the $C_{60}$ lattice. Work supported by Research Corporation Grant \# CC5240

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Author Institution: DEPARTMENT OF PHYSICS, OBERLIN COLLEGE

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