TUNNELING SPLITTINGS FOR THE NOMINAL OO STRETCHING AND OTHER VIBRATIONS OF TROPOLONE ISOTOPOMERS OBSERVED IN THE LOW FREQUENCY INFRARED SPECTRUM

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2007

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Ohio State University

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Fourier transform infrared spectra including resolved spectral doublets for many transitions are reported for gaseous tropolone(OH), tropolone(OD), and (18-O,18-O)tropolone(OH) in the 800 to $150 \wn$ spectral range. The known zero-point tunneling splitting values $\Delta_{0}$ = $0.974 \wn$ for tropolone(OH) (Tanaka et al.) and 0.$051 \wn$ for tropolone(OD) (Keske et al.) allow vibrational state-specific tunneling splittings $\Delta_{v}$ to be estimated for fundamentals including the three with the strongest OO stretching displacements [cf. for tropolone(OH) $\nub{13}$ = $435.22 \wn$ with $\Delta_{13}$ = $1.71 \wn$ = 1.76 $\Delta_{0}$, and for tropolone(OD) $\nub{13}$ = $429.631 \wn$ with $\Delta_{13}$ = $0.311 \wn$ = 6.10 $\Delta_{0}$]. In addition to revealing isotope-dependent $\Delta_{v}$ splittings the FTIR study demonstrates effects due to dynamic couplings and potential function anharmonicity. Vibrational reassignments are fostered and the pattern of $\Delta_{v}$ tunneling splitting values is interpreted to underscore the intrinsic multidimensionality of the tautomerization process in this nonrigid 15 atom molecule.

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Author Institution: Department of Chemistry and Biochemistry, Texas Tech University, Lubbock, TX 79409}; Wiley Environmental Molecular Sciences Laboratory, Pacific Northwest National Laboratory, Richland, WA 99352

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